低温反应体系

低温反应体系温度℃　冷却浴0碎冰-5->-20冰/盐-10.5乙二醇/干冰-12环庚烷/干冰-15苯甲醇/干冰-22四氯乙烯/干冰-22.8四氯化碳/干冰-251,3-二氯苯/干冰-29邻二甲苯/干冰-32间甲苯胺/干冰-41乙腈/干冰-42吡啶/干冰-47间二甲苯/干冰-56正辛烷/干冰-60异丙醚/干冰-77丙酮/干冰-77乙酸丁酯/干冰-83丙胺/干冰-83.6乙酸乙酯/液氮-89正丁醇/液氮-94己烷/液氮-94.6丙酮/液氮-95.1甲苯/液氮-98甲醇/液氮-100乙醚/干冰-104环己烷/液氮-116乙醇/液氮-116乙醚/液氮-131正五烷/液氮-160异戊烷/液氮-196液氮实验室低温反应浴（干冰或+溶剂）溶剂,低温,干冰,实验室干冰与以下试剂混合成糊状可达的低温:13op-Xylene12oDioxane6oCyclohexane5oBenzene2oFormamide-8.6oMethylsalicylate-9oHexane-2,5-dione-10.5oEthyleneglycol-11.9otert-Amylalcoho-12oCycloheptaneormethylbenzoate-15oBenzylalcohol-16.3on-Octanol-18o1,2-Dichlorobenzene-22oTetrachloroethylene-22.4oButylbenzoate-22.8oCarbontetrachloride-24.5oDiethylsulfate-25o1,3-Dichlorobenzene-29oo-Xyleneorpentachloroethane-30oBromobenzene-32om-Toluidine-32.6oDipropylketone-38oThiophene-41oAcetonitrile-42oPyridineordiethylketone-44oCyclohexylchloride-45oChlorobenzene-47om-Xylene-50oEthylmalonateorn-butylamine-52oBenzylacetateordiethylcarbito-55oDiacetone-56on-Octane-60oDi-isopropylether-73oTrichloroethyleneorisopropylacetate-74oo-Cymeneorp-cymene-77oButylacetate-79oIsoamylacetate-83oPropylamine-83.6oEthylacetate-86oMethylethylketone-89on-Butanol-90oNitroethane-91oHeptane-92on-Propylacetate-93o2-Nitropropaneorcyclopentane-94oEthylbenzeneorhexane-94.6oAcetone-95.1oToluene-97oCumene-98oMethanolormethylacetate-99oIsobutylacetate-104oCyclohexene-107oIsooctane-108o1-Nitropropane-116oEthanolordiethylether-117oIsoamylalcohol-126oMethylcyclohexane-131on-Pentane-160oIsopentaneSomeUsefulLaboratoryCoolingMixturesMixtureMixturetemperature(Centigrade)p-Xylene/Liquidnitrogen13p-Dioxane/Liquidnitrogen12Cyclohexane/Liquidnitrogen6Benzene/Liquidnitrogen5Formamide/Liquidnitrogen2Aniline/Liquidnitrogen-6Cycloheptane/Liquidnitrogen-12Benzonitrile/Liquidnitrogen-13Ethyleneglycol/Dryice-15o-Dichlorobenzene/Liquidnitrogen-18Tetrachloroetane/Liquidnitrogen-22Carbontetrachloride/Liquidnitrogen-23Carbontetrachloride/Dryice-23m-Dichlorobenzene/Liquidnitrogen-25Nitromethane/Liquidnitrogen-29o-Xylene/Liquidnitrogen-29Bromobenzene/Liquidnitrogen-30Iodobenzene/Liquidnitrogen-31Thiophene/Liquidnitrogen-383-Heptanone/Dryice-38Acetonitrile/Liquidnitrogen-41Pyridine/Liquidnitrogen-42Acetonenitrile/Dryice-42Chlorobenzene/Liquidnitrogen-45Cylcohexanone/Dryice-46m-Xylene/Liquidnitrogen-47n-Butylamine/Liquidnitrogen-50Diethylcarbitol/Dryice-52n-Octane/Liquidnitrogen-56Chloroform/Dryice-61(-77)Chloroform/Liquidnitrogen-63Methyliodide/Liquidnitrogen-66Carbitolacetate/Dryice-67t-Butylamine/Liquidnitrogen-68Ethanol/Dryice-72Trichloroethylene/Liquidnitrogen-73Butylacetate/Liquidnitrogen-77Acetone/Dryice-78Isopropanol/Dryice-78Isoamylacetate/Liquidnitrogen-79Acylonitrile/Liquidnitrogen-82Sulfurdioxide/Dryice-82Ethylacetate//Liquidnitrogen-84Ethylmethylketone/Liquidnitrogen-86Acrolein/Liquidnitrogen-88Nitroethane/Liquidnitrogen-90Heptane/Liquidnitrogen-91Cyclopentane/Liquidnitrogen-93Hexane/Liquidnitrogen-94Toluene/Liquidnitrogen-95Methanol/Liquidnitrogen-98Diethylether/Dryice-100n-Propyliodide/Liquidnitrogen-101n-Butyliodide/Liquidnitrogen-103Cyclohexane/Liquidnitrogen-104Isooctane/Liquidnitrogen-107Ethyliodide/Liquidnitrogen-109Carbondisulfide/Liquidnitrogen-110Butylbromide/Liquidnitrogen-112Ethylbromide/Liquidnitrogen-119Acetaldehyde/Liquidnitrogen-124Methylcyclohexane/Liquidnitrogen-126n-Pentane/Liquidnitrogen-1311,5-Hexadiene/Liquidnitrogen-141Isopentane/Liquidnitrogen-160体系建设